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Potassium Chlorate Lab

Posted by Jim Clark on 1st June and posted in Laboratory

Objective: To determine the number of oxygen atoms in a potassium chlorate molecule.

Potassium chlorate is a compound composed of potassium (K), chlorine (Cl), and oxygen (O). It melts at 368°C and decomposes at 400°C into the solid compound, potassium chloride (KCl), with molecular oxygen (O2) driven off.
potassium chlorate          potassium chloride + oxygen
KClOX =>             KCl             +     O2
Manganese dioxide is used as a catalyst in order to lower the energy of activation for the decomposition of potassium chlorate. The mass of the catalyst remains constant throughout the experiment.
Caution: Extreme caution must be used with potassium chlorate during handling and heating. Students who do not hear the lecture on safety precautions will have to get the lecture from the teacher at another time before they are permitted to do this experiment.

Procedure: Follow the procedure given in the paper, “Potassium Chlorate Lab Safety Precautions

Data (must be to two decimal places) trial 1 trial 2

mass of test tube + catalyst

mass of test tube, catalyst + KClOX

mass of test tube, catalyst + KCl

RESULTS
mass of KClOX added
mass of oxygen lost upon heating
atomic mass of oxygen
moles of oxygen (O) atoms
mass of KCl residue
molecular mass of KCl
moles of KCl
ratio of moles of O to moles of KCl : 1.00 : 1.00
simplest formula for potassium chlorate
balanced equation for the reaction (trial 1)
balanced equation for the reaction (trial 2)

Show calculation of moles of oxygen
atoms and moles of KCl molecules.

Show calculation of simplest whole
number ratio of O atoms to KCl molecules.

As soon as possible, insert your data from these trials into the class spreadsheet. This data will be needed by the class for later assignments. If the class is unable to analyze your data, you will not get full credit for your work.

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